Installation And Operation Specifications For Stainless Steel Reaction Kettle

Mar 05, 2024

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1. The high-pressure reactor should be placed indoors. When equipping multiple high-pressure reactors, they should be placed separately. Each operating room should have an exit directly leading to the outside or passage, and the equipment grounding point should be ensured to have good ventilation.
2. When installing the kettle cover, it is necessary to prevent the sealing surfaces between the kettle body and the kettle cover from colliding with each other. Carefully place the kettle lid in a fixed position on the kettle body, and when tightening the main nut, it must be tightened diagonally and symmetrically in multiple steps. Apply even force and do not allow the kettle lid to tilt to one side to achieve a good sealing effect.
3. At the joint of the positive and negative nuts, only the positive and negative nuts are allowed to be rotated, and the sealing surfaces of the two circular arcs must not be rotated relative to each other. When all nut pattern connections are assembled, lubricating oil should be applied.
4. The needle valve system is sealed with a thread. Simply rotate the valve needle gently and press the cover tightly to achieve a good sealing effect.
5. Rotate the rotating body on the kettle by hand to check if it operates flexibly.
6. The controller should be placed flat on the operating platform, with a working environment temperature of 10-40 ℃ and a relative humidity of less than 85%. The surrounding medium should not contain conductive dust or corrosive gases.
7. Check whether the movable parts and fixed contacts on the panel and back panel are normal, remove the cover, and check whether the connector contacts are loose, whether there is damage or rust caused by poor transportation and storage.
8. The controller should be reliably grounded.
9. Connect all wires, including power lines, electric furnace lines between the controller and the kettle, motor lines, temperature sensor and speedometer wires.
10. Close the "power" air main switch on the panel, and the digital display should show.
11. Set various parameters (such as upper limit alarm temperature, working temperature, etc.) on the digital display, then press the "heating" switch to turn on the electric furnace, and the indicator light on the "heating" switch will light up. Adjust the "pressure adjustment" knob to adjust the heating power of the electric furnace.
12. Press the "Mixing" switch to power on the mixing motor, and the indicator light on the "Mixing" switch will light up. Slowly turn the "Speed Control" knob to make the motor rotate slowly, observe whether the motor is rotating in the forward direction, and when there is no error, stop the machine, hang the belt, and restart.
13. After the operation is completed, it can be cooled naturally, cooled with water, or placed on a bracket for air cooling. After the temperature drops, release the pressurized gas inside the kettle to reduce the pressure to atmospheric pressure (the pressure gauge shows zero). Then, loosen the main nut symmetrically and evenly, remove the main nut, and carefully remove the kettle cover and place it on the bracket.
14. After each operation, the residue on the kettle body and lid should be removed. The main seal should be cleaned regularly and kept clean. It is not allowed to wipe it with hard objects or rough surfaces.

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